
Experiments in Physical Chemistry
by Shoemaker, David P.; Garland, Carl W.; Nibler, Joseph W.Rent Textbook
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Summary
Table of Contents
1 Introduction: Organization of the Book, Preparation for an Experiment, Execution of an Experiment, Safety, Recording of Experimental Data, Literature Work, Reports, Sample Reports, Special Projects2 Treatments of Experimental Data: A. Calculations and Presentation of Data: Significant Figures, Precision of Calculations, Analytical Methods, Numerical Methods, Graphs and Graphical Methods, Exercises; B. Uncertainties in Data and Results: Errors, Rejection of Discordant Data, Statistical Treatment of Random Errors, Significance Testing, Propagation of Errors, Case History of an Error Evaluation, Fundamental Limitations on Instrumental Precision, Summary, Exercises3 Use of Computer Software: Word Processors, Spreadsheets, Symbolic Mathematics Programs, Quantum Mechanical Programs, Exercises4 Gases: Gas Thermometry, Joule-Thomson Effect, Heat Capacity Ratios for Gases5 Transport Properties of Gases: Kinetic Theory of Transport Phenomena, Viscosity of Gases, Diffusion of Gases6 Thermochemistry: Principles of Calorimetry: Heats of Combustion, Strain Energy of the Cyclopropane Ring, Heats of Ionic Reaction7 Solutions: Partial Molal Volume, Cryoscopic Determination of Molecular Weight, Freezing-Point Depression of Strong and Weak Electrolytes, Chemical Equilibrium in Solution8 Phase Equilibria: Vapor Pressure of a Pure Liquid, Binary Liquid-Vapor Phase Diagram, Binary Solid-Liquid Phase Diagram, Liquid-Vapor Coexistence Curve and the Critical Point9 Electrochemistry: Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements10 Chemical Kinetics, Method of Initial Rate: Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics11 Surface Pheomena: Surface Tension of Solutions, Physical Adsorption of Gases12 Macromolecules: Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
3 Use of Computer Software: Word Processors, Spreadsheets, Symbolic Mathematics Programs, Quantum Mechanical Programs, Exercises4 Gases: Gas Thermometry, Joule-Thomson Effect, Heat Capacity Ratios for Gases5 Transport Properties of Gases: Kinetic Theory of Transport Phenomena, Viscosity of Gases, Diffusion of Gases6 Thermochemistry: Principles of Calorimetry: Heats of Combustion, Strain Energy of the Cyclopropane Ring, Heats of Ionic Reaction7 Solutions: Partial Molal Volume, Cryoscopic Determination of Molecular Weight, Freezing-Point Depression of Strong and Weak Electrolytes, Chemical Equilibrium in Solution8 Phase Equilibria: Vapor Pressure of a Pure Liquid, Binary Liquid-Vapor Phase Diagram, Binary Solid-Liquid Phase Diagram, Liquid-Vapor Coexistence Curve and the Critical Point9 Electrochemistry: Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements10 Chemical Kinetics, Method of Initial Rate: Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics11 Surface Pheomena: Surface Tension of Solutions, Physical Adsorption of Gases12 Macromolecules: Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
5 Transport Properties of Gases: Kinetic Theory of Transport Phenomena, Viscosity of Gases, Diffusion of Gases6 Thermochemistry: Principles of Calorimetry: Heats of Combustion, Strain Energy of the Cyclopropane Ring, Heats of Ionic Reaction7 Solutions: Partial Molal Volume, Cryoscopic Determination of Molecular Weight, Freezing-Point Depression of Strong and Weak Electrolytes, Chemical Equilibrium in Solution8 Phase Equilibria: Vapor Pressure of a Pure Liquid, Binary Liquid-Vapor Phase Diagram, Binary Solid-Liquid Phase Diagram, Liquid-Vapor Coexistence Curve and the Critical Point9 Electrochemistry: Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements10 Chemical Kinetics, Method of Initial Rate: Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics11 Surface Pheomena: Surface Tension of Solutions, Physical Adsorption of Gases12 Macromolecules: Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
7 Solutions: Partial Molal Volume, Cryoscopic Determination of Molecular Weight, Freezing-Point Depression of Strong and Weak Electrolytes, Chemical Equilibrium in Solution8 Phase Equilibria: Vapor Pressure of a Pure Liquid, Binary Liquid-Vapor Phase Diagram, Binary Solid-Liquid Phase Diagram, Liquid-Vapor Coexistence Curve and the Critical Point9 Electrochemistry: Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements10 Chemical Kinetics, Method of Initial Rate: Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics11 Surface Pheomena: Surface Tension of Solutions, Physical Adsorption of Gases12 Macromolecules: Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
9 Electrochemistry: Conductance of Solutions, Temperature Dependence of EMF, Activity Coefficients from Cell Measurements10 Chemical Kinetics, Method of Initial Rate: Iodine Clock, NMR Study of a Reversible Hydrolysis Reaction, Enzyme Kinetics: Inversion of Sucrose, Kinetics of the Decomposition of Benzenediazonium Ion, Gas-Phase Kinetics11 Surface Pheomena: Surface Tension of Solutions, Physical Adsorption of Gases12 Macromolecules: Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
11 Surface Pheomena: Surface Tension of Solutions, Physical Adsorption of Gases12 Macromolecules: Osmotic Pressure, Alcohol, Helix-Coil Transition in Polypeptides13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
13 Electric and Magnetic Properties: Dipole Moment of Polar Molecules in Solution, Dipole Moment of HCI Molecules in the Gas Phase, Magnetic Susceptibility, NMR Determination of Paramagnetic Susceptibility14 Spectroscopy: Absorption Spectrum of a Conjugated Dye, Infrared Spectroscopy: Vibrational Spectrum of SO2, Raman Spectroscopy: Vibrational Spectrum of CC14, Vibrational-Rotational Spectra of HC1 and DC1, Vibrational-Rotational Spectra of Acetylenes, Band Spectrum of Nitrogen, Absorption and Emission Spectra of Molecular Iodine, Electron Spin Resonance Spectroscopy, NMR Determination of Keto-Enol Equilibrium Constants, NMR Study of Gas Phase HC1-DBr Isotopic Exchange Reaction, Solid-State Lasers: Radiative Properties of Ruby Crystals15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
15 Solids: Determination of Crystal Structure by X-Ray Diffraction, Single Crystal X-Ray Diffraction with the Buerger Precession Camera, Lattic Energy of Solid Argon, Statistical Thermodynamics of Iodine Sublimation16 Computer Interfacing: Introduction, Types of Information Handled, Hardware, Software, Computer Programmin, Interfacing with Experiments17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
17 Electronic Devices and Measurements: Circuit Elements, Semiconductor Devices, Operational Amplifiers, Analog-to-digital Conversion, Digital Multimeters, Potentionmeter Circuits, Wheatstone Bridge Circuits, Capacitance Measurements18 Temperature: Temperature Scales, Triple-Point and Ice Point Cell, Thermometers, Temperature Control19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
19 Vacuum Techniques: Introduction, Theoretical Background, Pumping Speed for a System, Desorption and Virtual Leaks, Pumps, Vacuum Gauges, Miscellaneous Vacuum Components, Design of Vacuum Compenents, Design of Vacuum Lines, Leak Detection, Safety Considerations20 Instruments: Balances, Barometer, Oscilloscope, pH Meter, Polarimeter, Radiation Counters, Recorders and Plotters, Refractometers, Signal-Average Devices, Spectroscopic Components, Spectroscopic Instruments, Timing Devices, Westphal Balance21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
21 Miscellaneous Procedures: Volumetric Procedures, Purification Methods, Gas-Handling Procedures, Electrodes for Electrochemical Cells, Materials for Construction, Solders and Adhesives, Tubing Connections, ShopworkLeast Squares Fitting Procedures: Introduction, Foundations of Least Squares, Weights, Rejection of Discordant Data, Goodness of Fit, Compersion of Models, Uncertainties in the Parameters Summary of Procedures, Sample Least-Squares, CalculationAppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
AppendixesA: Glossary of SymbolsB: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
B: International System of Units and Concentration UnitsC: Safety, D: Literature WorkE: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
E: Research JournalsF: Numerical Methods of AnalysisG: Garomenter Corrections.
G: Garomenter Corrections.
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